Case number IPR2019-01425
Laboratory Corporation of America Holdings v. Quest Diagnostics Investments LLC et al. > Documents
| Date Field | Doc. No. | Party | Description |
|---|---|---|---|
| Apr 2, 2021 | 32 | patent_own | Patent Owner's Notice of Appeal Download |
| Feb 1, 2021 | 31 | board | Final Written Decision Determining All Challenged Claims Unpatentable 35 U.S.C. sec 318(a) Download |
| Jan 5, 2021 | 30 | board | Hearing Transcript Download |
| Oct 27, 2020 | 1051 | petitioner | Petitioner's Demonstratives Download |
| Oct 27, 2020 | 2026 | patent_own | Patent Owner's Demonstrative Exhibits Download |
| Oct 23, 2020 | 29 | board | Order Trial Hearing Download |
| Oct 1, 2020 | 28 | patent_own | Patent Owner's Sur-Reply Download |
| Sep 24, 2020 | 27 | patent_own | Patent Owner's Request for Oral Argument Download |
| Sep 22, 2020 | 26 | petitioner | Petitioner's Request for Oral Argument Download |
| Aug 20, 2020 | 1044 | petitioner | Deposition Transcript of Patrick M. Sluss taken February 12, 2020 in IPR2019-00738 Download |
| Aug 20, 2020 | 1045 | petitioner | Stockl et al., Specifications for Trueness and Precision of a Reference Measurement System for Serum/Plasma 25-Hydroxyvitamin D. Analysis, Clin. Chim. Acta 408:8-13 (2009) Download |
| Aug 20, 2020 | 1046 | petitioner | Declaration of Steve Lock dated August 12, 2019 Download |
| Aug 20, 2020 | 1047 | petitioner | Declaration of Dr. Robert Voyksner dated February 28, 2020 Download |
| Aug 20, 2020 | 1048 | petitioner | Declaration of Patrick M. Sluss, Ph.D. in IPR2019-00738 Download |
| Aug 20, 2020 | 1049 | petitioner | Deposition Transcript of Patrick M. Sluss, Ph.D. on July 27, 2020 Download |
| Aug 20, 2020 | 1050 | petitioner | Landmann et al., Soluable CD14 Activates Monocytic Cells Independently of Lipopolysaccharide, Infection and Immunity 66(5):2264-71 (1998) Download |
| Aug 20, 2020 | 25 | petitioner | Petitioner's Reply to Patent Owner's Response Download |
| Jun 25, 2020 | 24 | petitioner | Petitioner's Notice of Deposition of Patrick M. Sluss, PH.D. Under 37 C.F.R. section 42.53 Download |
| Jun 5, 2020 | 23 | PETITIONER UPDATED EXHIBIT LIST Download | |
| Jun 4, 2020 | 21 | Download | |
| Jun 4, 2020 | 22 | ORDER Granting Petitioner's Motion to Submit Supplemental Information Download | |
| Jun 4, 2020 | 3002 | Ex 3002 Download | |
| May 28, 2020 | 1042 | Declaration of Christopher Butler with attached Exhibit A from Zorbax HPLC Columns Download | |
| May 28, 2020 | 1043 | Declaration of Christopher Butler with attached Exhibits A and B from ASMS Download | |
| May 28, 2020 | 19 | Motion to Submit Supplemental Information Download | |
| May 28, 2020 | 20 | Patent Owner's Response Download | |
| May 28, 2020 | 2004 | May 14, 2020 Deposition Transcript of Robert L. Fitzgerald, Ph.D. Download | |
| May 28, 2020 | 2005 | Woods, G. N., et al., A young woman with recurrent gestational hypercalcemia and acute pancreatitis caused by CYP24A1 deficiency. Journal of Bone and Mineral Research, 31(10): 1841-1844 (2016). Download | |
| May 28, 2020 | 2006 | Kim, S., et al., How much is too much? Two contrasting cases of excessive vitamin D supplementation. Clinica Chimica Acta, 473: 35-38 (2017). Download | |
| May 28, 2020 | 2007 | Coburn, J. W., Metabolism and action of the hormone vitamin D: its relation to diseases of calcium homeostasis. Western Journal of Medicine, 121(1), 22 (1974). Download | |
| May 28, 2020 | 2008 | Download | |
| May 28, 2020 | 2009 | Declaration of Patrick M. Sluss, Ph.D. Download | |
| May 28, 2020 | 2010 | File History for U.S. Patent. No. 7,972,867. Download | |
| May 28, 2020 | 2011 | Colston, K. W., et al. Feedback regulation of vitamin D metabolism by 1, 25-dihydroxycholecalciferol. Biochemical Journal 164.1:83-89 (1977). Download | |
| May 28, 2020 | 2012 | Boyle, I.T., et al. The biological activity and metabolism of 24, 25-dihydroxyvitamin D3. Journal of Biological Chemistry 248.12: 4174-4180 (1973). Download | |
| May 28, 2020 | 2013 | Nemere, I., Apparent nonnuclear regulation of intestinal phosphate transport: effects of 1, 25-dihydroxyvitamin D3, 24, 25-dihydroxyvitamin D3, and 25-hydroxyvitamin D3. Endocrinology 137.6:2254-2261 (1996). Download | |
| May 28, 2020 | 2014 | Norman, A.W. From vitamin D to hormone D: fundamentals of the vitamin D endocrine system essential for good health. The American journal of clinical nutrition 88.2: 491S-499S (2008). Download | |
| May 28, 2020 | 2015 | Higashi, T., et al. Download | |
| May 28, 2020 | 2016 | van den Ouweland, JMW. Analysis of vitamin D metabolites by liquid chromatography-tandem mass spectrometry. TrAC Trends in Analytical Chemistry 84:117-130 (2016). Download | |
| May 28, 2020 | 2017 | Galior, K., et al. 10 years of 25-hydroxyvitamin-D testing by LC-MS/MS-trends in vitamin-D deficiency and sufficiency. Bone reports 8:268-273 (2018). Download | |
| May 28, 2020 | 2018 | Ishimura, E., et al. Serum levels of 1, 25-dihydroxyvitamin D, 24, 25-dihydroxyvitamin D, and 25-hydroxyvitamin D in nondialyzed patients with chronic renal failure. Kidney international 55.3: 1019-1027 (1999). Download | |
| May 28, 2020 | 2019 | Le Goff, C., et al. Measurement of circulating 25-hydroxyvitamin D: a historical review. Practical laboratory medicine 2:1-14 (2015). Download | |
| May 28, 2020 | 2020 | Fraser, William D., et al. Vitamin D assays: past and present debates, difficulties, and developments. Calcified tissue international 92.2: 118-127 (2013). Download | |
| May 28, 2020 | 2021 | Ding, Shujing, et al., Quantitative determination of vitamin D metabolites in plasma using UHPLC-MS/MS. Analytical and bioanalytical chemistry 398.2: 779-789 (2010). Download | |
| May 28, 2020 | 2022 | Ornoy, A., et al. 24, 25-Dihydroxyvitamin D is a metabolite of vitamin D essential for bone formation. Nature 276.5687:517-519 (1978). Download | |
| May 28, 2020 | 2023 | Weisman, Y., et al. Serum 24, 25-dihydroxyvitamin D and 25-hydroxyvitamin D concentrations in femoral neck fracture. British medical journal 2.6146: 1196 (1978). Download | |
| May 28, 2020 | 2024 | Niessen, W. M. A. Thermospray Ionization in Mass Spectrometry. Elsevier Reference Module Chemical, Molecular Sciences and Engineering. (2013). Download | |
| May 28, 2020 | 2025 | Memorandum Order addressing claim construction in Civil Action No. 1:18-cv-01436 (MN) on January 14, 2020. Download | |
| Apr 30, 2020 | 18 | Patent Owner's Second Notice of Deposition of Dr. Robert L. Fitzgerald Download | |
| Mar 23, 2020 | 17 | Patent Owner's Notice of Cancellation of Deposition of Dr. Robert L. Fitzgerald Download | |
| Mar 20, 2020 | 16 | Joint Stipulation to Adjust the Scheduling Order Download | |
| Mar 11, 2020 | 15 | Patent Owner's Notice of Deposition of Dr. Robert L. Fitzgerald Download | |
| Mar 9, 2020 | 14 | Order - 37 CFR 42.123(a) Download | |
| Mar 9, 2020 | 3001 | Ex. 3001 Download | |
| Feb 20, 2020 | 13 | Patent Owner's Objections to Evidence Download | |
| Feb 14, 2020 | 12 | Petitioner's Updated Mandatory Notice Pursuant to 37 C.F.R. Section 42.8 Download | |
| Feb 10, 2020 | 11 | Patent Owner's Updated Mandatory Notices Download | |
| Feb 6, 2020 | 10 | Scheduling Order Download | |
| Feb 6, 2020 | 9 | Decision - Instituting Inter Partes Review Download | |
| Nov 12, 2019 | 8 | ORDER Granting Patent Owner's Motion for Pro Hac Vice Admission of Thomas H. Wintner Download | |
| Nov 7, 2019 | 2003 | File History for U.S. Patent No. 7,745,226 Download | |
| Nov 7, 2019 | 2002 | Joint Claim Construction Chart Ex. A filed in Civil Action No. 1:18-cv-01436 (MN) on September 25, 2019 Download | |
| Nov 7, 2019 | 7 | Patent Owner's Preliminary Response Download | |
| Aug 15, 2019 | 2001 | Declaration of Thomas H. Wintner in Support of Motion for Pro Hac Vice Admission Download | |
| Aug 15, 2019 | 6 | Patent Owner's Unopposed Motion for Pro Hac Vice Admission of Thomas H. Wintner Download | |
| Aug 12, 2019 | 4 | Patent Owner's Power of Attorney Download | |
| Aug 12, 2019 | 5 | Patent Owner's Mandatory Notices Download | |
| Aug 7, 2019 | 3 | Notice of Accord Filing Date Download | |
| Jul 29, 2019 | 1 | Petition for Inter Partes Review Download | |
| Jul 29, 2019 | 1001 | U.S. Patent. No. 8,101,427 to Clarke et al. Download | |
| Jul 29, 2019 | 1002 | Declaration of Robert L. Fitzgerald, Ph.D., DABCC Download | |
| Jul 29, 2019 | 1003 | File History for U.S. Patent. No. 8,101,427 to Clarke et al. Download | |
| Jul 29, 2019 | 1004 | Voyksner and Lee, Improvements in LC/Electrospray Ion Trap Mass Spectrometry Performance Using an Off-Axis Nebulizer, Anal. Chem. 71:1441-47 (1999) Download | |
| Jul 29, 2019 | 1005 | Kissmeyer and Sonne, Sensitive Analysis of 25-Dihydroxyvitamin D3 in Biological Fluids by Liquid Chromatography-Tandem Mass Spectrometry, J. Chromatography A 935:93-103 (2001) Download | |
| Jul 29, 2019 | 1006 | Kamao et al., C-3 Epimerization of Vitamin D3 Metabolites and Further Metabolism of C-3 Epimers, Manuscript M311473200, JBC Papers in Press, 1-31 (2004) Download | |
| Jul 29, 2019 | 1007 | Watson et al., Analysis of Vitamin D and Its Metabolites Using Thermospray Liquid Chromatography/Mass Spectrometry, Biomedical Chromatography 5:153-60 (1991) Download | |
| Jul 29, 2019 | 1008 | Rainbow et al., The Analysis of Vitamin D Analogues by Atmospheric Pressure Ionization Coupled to Triple Quadrupole Mass Spectrometry, Poster No. M-045, Proceedings of the 51st ASMS Conference on Mass Spectrometry and Allied Topics, Montreal, Canada Download | |
| Jul 29, 2019 | 1009 | Vogeser, Liquid Chromatography-Tandem Mass Spectrometry Application in the Clinical Laboratory, Clin.Chem. Lab. Med. 41(2):117-26 (2003) Download | |
| Jul 29, 2019 | 1010 | Interview Summary dated January 28, 2009 for U.S. Patent No. 7,774,226 Download | |
| Jul 29, 2019 | 1011 | Patent Owner Response dated April 7, 2009 for U.S. Patent No. 7,774,226 Download | |
| Jul 29, 2019 | 1012 | Office Action dated April 12, 2010 for U.S. Patent No. 7,972,867 Download | |
| Jul 29, 2019 | 1013 | Patent Owner Response dated July 8, 2010 for U.S. Patent No. 7,972,867 Download | |
| Jul 29, 2019 | 1014 | Glenville Jones and Hugh L.J. Makin, Vitamin Ds, Metabolites and Analogues, Chapter 2 in Modern Chromatographic Analysis of Vitamins, 87-153 (Leenheer, Lambert & Van Bocxlaer, eds., 3rd ed. 2000) Download | |
| Jul 29, 2019 | 1015 | Download | |
| Jul 29, 2019 | 1016 | Lagan et al., Liquid Chromatography Tandem Mass Spectrometry Applied to the Analysis of Natural and Synthetic Steroids in Environmental Waters, Analytical Letters 34(6):913-26 (2001) Download | |
| Jul 29, 2019 | 1017 | Declaration of Catherine Vassilkova Download | |
| Jul 29, 2019 | 1018 | Declaration of Andrew Hoofnagle, M.D., Ph.D. Download | |
| Jul 29, 2019 | 1019 | Declaration of Patrick Gordis (for Watson) Download | |
| Jul 29, 2019 | 1020 | Declaration of Christopher Butler Download | |
| Jul 29, 2019 | 1021 | Declaration of Dr. Robert Voyksner Download | |
| Jul 29, 2019 | 1022 | Declaration of Patrick Gordis (for Vogeser) Download | |
| Jul 29, 2019 | 1023 | National Library of Medicine, PubChem Computed Properties for Calcitriol Download | |
| Jul 29, 2019 | 1024 | Zimmer et al., Comparison of Turbulent-Flow Chromatography with Automated Solid-Phase Extraction in 96-Well Plates and Liquid-Liquid Extraction Used as Plasma Sample Preparation Techniques for Liquid Chromatography-Tandem Mass Spectrometry Download | |
| Jul 29, 2019 | 1025 | Couchman, Turbulent Flow Chromatography in Bioanalysis: A Review, Biomed. Chromatography 26:892-905 (2012) Download | |
| Jul 29, 2019 | 1026 | Hollis and Napoli, Improved Radioimmunoassay for Vitamin D and Its Use in Assessing Vitamin D Status, Clin. Chem. 31(11):1815-19 (1985) Download | |
| Jul 29, 2019 | 1027 | A. Michael Parfitt, Osteomalacia and Related Disorders,in Metabolic Bone Disease and Clinically Related Disorders, 329-96 (Aviolo, Krane, eds., 3rd ed.1997) Download | |
| Jul 29, 2019 | 1028 | Trivedi et al., Effect of Four Monthly Oral Vitamin D3 (Cholecalciferol) Supplementation of Fractures and Mortality in Men and Women Living in the Community: Randomised Double Blind Controlled Trial, BMJ 326:469-74 (2003) Download | |
| Jul 29, 2019 | 1029 | Armas et al., Vitamin D2 is Much Less Effective than Vitamin D3 in Humans, J. Clin. Endocrinol. & Metab., 89:5387-91 (2004) Download | |
| Jul 29, 2019 | 1030 | Food and Nutrition Board, Institute of Medicine, Dietary Reference Intakes for Calcium, Magnesium, Phosphorus, Vitamin D and Fluoride 250-87 (National Academy Press 1997) Download | |
| Jul 29, 2019 | 1031 | Kissmeyer et al., Determination of the Vitamin D Analog EB 1089 (Seocalcitol) in Human and Pig Serum Using Liquid Chromatography-Tandem Mass Spectrometry, J. Chromatog. B, 740:117-28 (2000) Download | |
| Jul 29, 2019 | 1032 | Herbert and Johnstone, Mass Spectrometry Basics 225-35, 245-52, 261-68, and 413-15 (CRC Press LLC, 2002) Download | |
| Jul 29, 2019 | 1033 | Fitzgerald et al., Broad Spectrum Drug Identification Directly from Urine, Using Liquid Chromatography-Tandem Mass Spectrometry, Clin. Chem. 45:1224-34 (1999) Download | |
| Jul 29, 2019 | 1034 | Fitzgerald et al., Comparison of an Ion Trap and a Quadrupole Mass Spectrometer Using Diazepam as a Model Compound, J. Analytical Toxicology 21:445-50 (1997) Download | |
| Jul 29, 2019 | 1035 | Kamao et al., C-3 Epimerization of Vitamin D3 Metabolites and Further Metabolism of C-3 Epimers, J. Biol. Chem. 279:15897-907 (2004) Download | |
| Jul 29, 2019 | 1036 | Ma and Kim, Determination of Steroids by Liquid Chromatography/Mass Spectrometry, J. Am. Soc. Mass Spectrom. 8:1010-20 (1997) Download | |
| Jul 29, 2019 | 1037 | Fred W. McLafferty & Frantisek Turecek, Interpretation of Mass Spectra 349 (4th ed. 1993) Download | |
| Jul 29, 2019 | 1038 | Francis A. Carey, Stereochemistry,in Organic Chemistry 259-301 (McGraw-Hill, 4th ed. 2000) Download | |
| Jul 29, 2019 | 1039 | Davankov, Analytical Chiral Separation Methods (IUPAC Recommendations 1997), Pure and Applied Chemistry 69:1467-74 (1997) Download | |
| Jul 29, 2019 | 1040 | Mac-Mod Zorbax HPLC Columns Product Bulletin Download | |
| Jul 29, 2019 | 1041 | Declaration of Dr. Russell Grant Download | |
| Jul 29, 2019 | 2 | Power of Attorney Download |
