Date Field | Doc. No. | Party | Description |
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Oct 1, 2020 | 22 | board | Termination Decision Document Download |
Sep 23, 2020 | 21 | petitioner | Petitioner's Notice of Deposition of Christopher J. Welch, PH.D Under 37 C.F.R. Section 42.53 Download |
Sep 18, 2020 | 20 | petitioner | Joint Request to File Covenant Not to Sue as Business Confidential Information Pursuant to 35 U.S.C. Section 317(b) and 37 C.F.R. Section 42.74(c) Download |
Sep 18, 2020 | 19 | petitioner | Joint Motion to Terminate Pursuant to 35 U.S.C. Section 317 and 37 C.F.R. Section 42.74 Download |
Sep 18, 2020 | 1039 | petitioner | Joint Stipulation and Order of Voluntary Dismissal with Prejudice Download |
Jul 21, 2020 | 18 | petitioner | Petitioner's Objections to Evidence Submitted with Patent Owner's Response Download |
Jul 14, 2020 | 2017 | patent_own | NIH PubChem entry for 1,4-Phthalazinedione structure, available at https://pubchem.ncbi.nlm.nih.gov/compound/1_4-Phthalazinedione (last accessed July 10, 2020). Download |
Jul 14, 2020 | 2016 | patent_own | van den Ouweland, JMW. Analysis of vitamin D metabolites by liquid chromatography-tandem mass spectrometry. TrAC Trends in Analytical Chemistry 84:117-130 (2016). Download |
Jul 14, 2020 | 2015 | patent_own | Aronov et al., Metabolic profiling of major vitamin D metabolites using Diels-Alder derivatization and ultra-performance liquid chromatography-tandem mass spectrometry, Anal. Bioanal. Chem. 391(5):1917-1930 (2008). Download |
Jul 14, 2020 | 2014 | patent_own | SciFinder literature search results for 4'-carboxyphenyl-TAD. Download |
Jul 14, 2020 | 2013 | patent_own | Download |
Jul 14, 2020 | 2012 | patent_own | Knapp, D.R., Handbook of Analytical Derivatization Reactions, John Wiley & Sons. (1979). Download |
Jul 14, 2020 | 2011 | patent_own | Memorandum Order addressing claim construction in Civil Action
No. 1:18-cv-01436 (MN) on January 14, 2020. Download |
Jul 14, 2020 | 2010 | patent_own | March J., Advanced Organic Chemistry, 3rd Ed., John Wiley & Sons. (1985). Download |
Jul 14, 2020 | 2009 | patent_own | Download |
Jul 14, 2020 | 2008 | patent_own | July 1, 2020 Deposition Transcript of Robert L. Fitzgerald,
Ph.D. Download |
Jul 14, 2020 | 2007 | patent_own | Karlson, P., et al., IUPAC-IUB Joint Commission on Biochemical Nomenclature (JCBN): nomenclature of vitamin D--recommendations 1981, Eur. J. Biochem. (1982) Download |
Jul 14, 2020 | 2006 | patent_own | June 30, 2020 Deposition Transcript of Robert D. Voyksner,
Ph.D. Download |
Jul 14, 2020 | 17 | patent_own | Patent Owner's Response Download |
Jun 16, 2020 | 16 | | Patent Owner's Notice of Deposition of Dr. Robert L. Fitzgerald Download |
Jun 16, 2020 | 15 | | Patent Owner's Notice of Deposition of Dr. Robert Voyksner Download |
May 14, 2020 | 14 | | Joint Stipulation to Adjust the Scheduling Order Download |
Mar 20, 2020 | 13 | | Scheduling Order Download |
Mar 20, 2020 | 12 | | Trial Instituted Document Download |
Feb 14, 2020 | 11 | | Petitioner's Updated Mandatory Notice Pursuant to 37 C.F.R. Section 42.8 Download |
Dec 24, 2019 | 2005 | | Loudon, M.G., Organic Chemistry, 3rd ed. (1995) Download |
Dec 24, 2019 | 2004 | | Vreeken, R.J. et al., On-line post-column Diels-Alder derivatization for the determination of vitamin D3 and its metabolites by liquid chromatography/thermospray mass spectrometry, Biol. Mass. Spec., 22, 621-632 (1993) Download |
Dec 24, 2019 | 2003 | | Joint Claim Construction Chart - Exhibit A filed in Civil Action No. 1:18-cv-01436-MN Download |
Dec 24, 2019 | 2002 | | Download |
Dec 24, 2019 | 10 | | Patent Owner's Preliminary Response Download |
Dec 20, 2019 | 9 | | Download |
Oct 22, 2019 | 8 | | Patent Owner's Unopposed Motion for Pro Hac Vice Admission of Thomas H. Wintner Download |
Oct 22, 2019 | 2001 | | Declaration of Thomas H. Wintner in Support of Motion for Pro Hac Vice Admission Download |
Sep 30, 2019 | 7 | | NOTICE OF ACCEPTING CORRECTED PETITION Download |
Sep 27, 2019 | 6 | | Patent Owner's Mandatory Notices Download |
Sep 27, 2019 | 5 | | Patent Owner's Power of Attorney Download |
Sep 26, 2019 | 4 | | Corrected Petition for Inter Partes Review Download |
Sep 26, 2019 | 1006 | | [Replacement] Higashi et al., Characterization of Urinary Metabolites of Vitamin D3 in Man under Physiological Conditions Using Liquid Chromatography-Tandem Mass Spectrometry, J. Pharm. Biomed. Anal. 29:947-55 (2002) Download |
Sep 25, 2019 | 3 | | Notice of Accord Filing Date Download |
Sep 17, 2019 | 1035 | | Creaser et al., Immunoaffinity Chromatography Combined On-Line with High Performance Liquid Chromatography-Mass Spectrometry for the Determination of Corticosteroids, J. Chromatography A 794:37-43 (1998) Download |
Sep 17, 2019 | 1006 | | Higashi et al., Characterization of Urinary Metabolites of Vitamin D3 in Man under Physiological Conditions Using Liquid Chromatography-Tandem Mass Spectrometry, J. Pharm. Biomed. Anal. 29:947-55 (2002) Download |
Sep 17, 2019 | 1011 | | Higashi et al., Electron-Capturing Derivatization of Neutral Steroids for Increasing Sensitivity in Liquid Chromatography/Negative Atmospheric Pressure Chemical Ionization-Mass Spectrometry, Anal. Sci. 18:1301-07 (2002) Download |
Sep 17, 2019 | 1032 | | Fitzgerald et al., Comparison of an Ion ¿¿¿Trap and a Quadrupole Mass Spectrometer using Diazepam as a Model Compound, J. Analytical Toxicology, 21:445-50 (1997) Download |
Sep 17, 2019 | 1 | | Petition for Inter Partes Review Download |
Sep 17, 2019 | 1019 | | Declaration of Patrick Gordis (for Higashi) Download |
Sep 17, 2019 | 1025 | | A. Michael Parfitt, Osteomalacia and Related Disorders, in Metabolic Bone Disease and Clinically Related Disorders,329-96 (Aviolo, Krane, eds., 3rd ed. 1997) Download |
Sep 17, 2019 | 1030 | | Herbert and Johnstone, Mass Spectrometry Basics 225-35, 245-52, 261-68, and 413-15 (CRC Press LLC, 2002) Download |
Sep 17, 2019 | 1003 | | File History for U.S. Patent No. 7,972,868 to Holmquist et al. Download |
Sep 17, 2019 | 1014 | | Declaration of Dr. Robert Voyksner Download |
Sep 17, 2019 | 1023 | | Kissmeyer and Sonne, Sensitive Analysis of 1,25-Dihydroxyvitamin D3 in Biological Fluids by Liquid Chromatography-Tandem Mass Spectrometry, J. Chromatography A 935:93-103 (2001) Download |
Sep 17, 2019 | 1033 | | Voyksner and Lee, Improvements in LC/Electrospray Ion Trap Mass Spectrometry Performance Using an Off-Axis Nebulizer, Anal. Chem. 71:1441-47 (1999) Download |
Sep 17, 2019 | 1024 | | Rainbow et al., The Analysis of Vitamin D Analogues by Atmospheric Pressure Ionization Coupled to TripleQuadrupole Mass Spectrometry, Poster No. M-045, Proceedings of the 51st ASMS Conference on Mass Spectrometry and Allied Topics, Montreal, Canada Download |
Sep 17, 2019 | 1008 | | Kobayashi et al., Production of a Group-Specific Antibody to 1 a,25-Dihydroxyvitamin D and Its Derivatives Having the 1 a,3 b-Dihydroxylated A-Ring Structure, Steroids 59:404-11 (1994) Download |
Sep 17, 2019 | 1031 | | Fitzgerald et al., Broad Spectrum Drug Identification Directly from Urine, Using Liquid Chromatography-Tandem Mass Spectrometry, Clin. Chem., 45:1224-34 (1999) Download |
Sep 17, 2019 | 1004 | | Tsugawa et al., Determination of 25-Hydroxyvitamin D in Human Plasma Using High-Performance Liquid Chromatography-Tandem Mass Spectrometry, Anal. Chem. 77:3001-07 (2005) Download |
Sep 17, 2019 | 1018 | | Declaration of Patrick Gordis (for Yeung) Download |
Sep 17, 2019 | 1013 | | Kobayashi et al., Tandem Immunoaffinity Chromatography, J. Steroid Biochem. Molec. Biol. 54:217-26 (1995) (Kobayashi 1995) Download |
Sep 17, 2019 | 1021 | | Fitzgerald and Herold, Serum Total Testosterone: Immunoassay Compared with Negative Chemical Ionization Gas Chromatography Mass Spectrometry, Clin. Chem. 42(5):749-55 (1996) Download |
Sep 17, 2019 | 1015 | | Vogeser, Liquid Chromatography-Tandem Mass Spectrometry Application in the Clinical Laboratory, Clin. Chem. Lab. Med. 41(2):117-26 (2003) Download |
Sep 17, 2019 | 1017 | | Declaration of Patrick Gordis (for Tsugawa) Download |
Sep 17, 2019 | 1034 | | Glenville Jones and Hugh L.J. Makin, ¿¿¿Vitamin Ds: Metabolites and Analogues,¿¿¿ Chapter 2 in Modern Chromatographic Analysis of Vitamins, 87-153 (Leenheer, Lambert & Van Bocxlaer, eds., 3rd ed. 2000) Download |
Sep 17, 2019 | 1022 | | Legrand et al., Measurement of plasma testosterone by gas chromatography-negative-ion mass spectrometry using pentafluoropropionic derivatives, J. Chromatog. 663:187-92, 189 (1995) Download |
Sep 17, 2019 | 1027 | | Armas et al., Vitamin D2 is Much Less Effective than Vitamin D3 in Humans, J. Clin. Enodcrinol. & Metab., 89:5387-91(2004) Download |
Sep 17, 2019 | 1005 | | Yeung et al., Characterization of Vitamin D3 Metabolites Using Continuous-Flow Fast Atom Bombardment Tandem Mass Spectrometry and High-Performance Liquid Chromatography, J. Chromatography 645:115-23 (1993) Download |
Sep 17, 2019 | 1029 | | Kissmeyer et al., Determination of the Vitamin D Analog EB 1089 (Seocalcitol) in Human and Pig Serum Using Liquid Chromatography-Tandem Mass Spectrometry, J. Chromatog. B, 740:117-28 (2000) Download |
Sep 17, 2019 | 2 | | Power of Attorney Download |
Sep 17, 2019 | 1006 | | Higashi et al., Characterization of Urinary Metabolites of Vitamin D3 in Man under Physiological Conditions Using Liquid Chromatography-Tandem Mass Spectrometry, J. Pharm. Biomed. Anal. 29:947-55 (2002) Download |
Sep 17, 2019 | 1037 | | National Library of Medicine, PubChem Computed Properties for Calcitriol Download |
Sep 17, 2019 | 1001 | | U.S. Patent No. 7,972,868 to Holmquist et al. Download |
Sep 17, 2019 | 1016 | | Honour, High-Performance Liquid Chromatography for Hormone Assay Chapter 2 in Methods in Molecular Biology: Hormone Assays in Biological Fluids, 25-51 (M.J. Wheeler & J.S.M. Hutchinson, eds., 2006) Download |
Sep 17, 2019 | 1009 | | U.S. Patent No. 6,787,660 to Armbruster et al. Download |
Sep 17, 2019 | 1002 | | Declaration of Robert L. Fitzgerald, Ph.D., DABCC Download |
Sep 17, 2019 | 1012 | | Higashi et al., Application of 4-(4-Nitrophenyl)-1,2,4-triazoline-3,5-dione to Analysis of 25-Hydroxyvitamin D3 in Human Plasma by Liquid Chromatography/Electron Capture Atmospheric Pressure Chemical Ionization-Mass Spectrometry, Anal. Sci. 19:941-43 Download |
Sep 17, 2019 | 1036 | | Hollis and Napoli, Improved Radioimmunoassay for Vitamin D and Its Use in Assessing Vitamin D Status, Clin. Chem. 31(11):1815-19 (1985) Download |
Sep 17, 2019 | 1007 | | U.S. Patent No. 6,399,796 to Schwartz Download |
Sep 17, 2019 | 1010 | | Reserved Download |
Sep 17, 2019 | 1020 | | Declaration of Patrick Gordis (for Kobayashi) Download |
Sep 17, 2019 | 1026 | | Trivedi et al., Effect of Four Monthly Oral Vitamin D3 (Cholecalciferol) Supplementation of Fractures and Mortalityin Men and Women Living in the Community: Randomised Double Blind Controlled Trial, BMJ 326:469-74 (2003) Download |
Sep 17, 2019 | 1028 | | Food and Nutrition Board, Institute of Medicine, Dietary Reference Intakes For Calcium, Magnesium, Phosphorus,Vitamin D and Fluoride, 250-287 (National Academy Press,
1997) Download |